Polarization-Modulated Infrared Reflection Absorption Spectroscopy

This PMIRRAS technique exploits the fact that when infrared light is reflected by a conducting surface, the amplitude of the s- and p-polarized electric field vectors near the surface differ strongly. The s-polarized electric field amplitude is approximately zero within a distance of the order of one wavelength of the surface, whereas the p-polarized electric field amplitude is larger in this region.
Therefore, if a conducting substrate bears a film whose thickness is much less than the wavelength of the infrared light, then reflected p-polarized light is modified by the absorption spectrum of the film, whereas reflected s-polarized light will contain no signal from the film. The p-polarized reflected light spectrum can thus be treated as the signal with the s-polarized spectrum being used as the background to be subtracted.

PM-IRRAS instruments effectively achive this subtraction by rapidly modulating the polarization and using a lock-in amplifier to extract the signal. IRRAS spectra with a very low signal- to-noise ratio can thus be obtained.